Principles and Practice of Variable Pressure Scanning Electron Microscopy (VPSEM)

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83,90 

Environmental Scanning Electron Microscopy (VP-ESEM), RMS – Royal Microscopical Society

ISBN: 0470065400
ISBN 13: 9780470065402
Autor: Stokes, Debbie
Verlag: Wiley-VCH GmbH
Umfang: 224 S.
Erscheinungsdatum: 14.11.2008
Auflage: 1/2008
Produktform: Gebunden/Hardback
Einband: GEB
Artikelnummer: 1045458 Kategorie:

Beschreibung

Scanning electron microscopy (SEM) is a technique of major importance and is widely used throughout the scientific and technological communities. The modern SEM is capable of resolution on the order of a few Angstroms (i.e. sub-nanometer), subject to the limits of electron-specimen interactions. However, for a long time it has been apparent that the high vacuum SEM needed to develop in respects other than increased resolution. Hence the advent of SEMs that utilise a gas for image formation while simultaneously providing charge stabilisation for electrically non-conductive specimens and/or a suitable environment for materials and experiments involving water. This text outlines the principles and applications in a generic way, applicable to readers familiar with any of the types of VP-ESEM on the market, irrespective of manufacturer The book addresses various aspects of the topic in six chapters. * Chapter 1 A brief historical overview contains background information charting the development and growth of the technique and its underlying principles * Chapter 2 Principles of SEM gives an overview of various aspects of the conventional high vacuum SEM, in preparation for later chapters covering the greater variety of operating conditions associated with the VPESEM * Chapter 3 General principles of VPESEM: utilising a gas reviews the basic scientific principles of signal formation and collection in a gaseous environment, including specimen stability as a function of water vapour pressure and/or temperature. * Chapter 4 Imaging and analysis in the VPESEM: the influence of a gas looks at the properties and effects of different gases, pressures and primary electron energies, with particular attention to electron scattering and its effects on imaging and microanalysis * Chapter 5 Imaging uncoated specimens in the VPESEM briefly looks at the pros and cons of putting nativestate materials in the VPESEM, such as primary electron beam penetration, radiation damage and, crucially, the properties of materials in an electric field and the influence of gaseous positive ions * Chapter 6 A lab in a chamber in situ methods in VPESEM and other applications concludes the book with a survey of dynamic experiments such as: tensile testing, vapourdeposition of nanostructures, oxidation and reduction,lithography, ice crystallization and wetting of surfaces, to name a few, as well as unique imaging methods, plus an extensive review of the literature covering both hard and soft materials. This book is intended as a guide to help those that are just starting out with VP-ESEM, as well as those with more experience looking to gain a deeper appreciation of the concepts.

Inhaltsverzeichnis

Contents Chapter 1 -A brief historical overview 1.1 Scanning electron microscopy 1.2 The development of imaging in a gas environment Chapter 2 -Principles of SEM 2.1 Introduction 2.2 Electron sources 2.3 Electron optics 2.4 Signals and detection 2.5 Practical aspects of electron beam irradiation 2.6 the sem in operation Chapter 3 -General principles of VP-ESEM: utilising a gas 3.1 Introduction 3.2 VP-ESEM instrumentation 3.3 Signal generation in a gas 3.4 Imaging with water vapour Chapter 4 -Imaging and analysis in the VP-ESEM: the influence of a gas 4.1 Introduction 4.2 Background to theoretical calculations 4.3 Which gas? 4.4 Exploring the gas path length 4.5 How much gas? 4.6 X-ray microanalysis in the VP-ESEM Chapter 5 -Imaging uncoated specimens in the VP-ESEM 5.1 Introduction 5.2 Electronic structure 5.3 Factors affecting secondary electron emission 5.4 The influence of the specimen on the system 5.5 Time- and temperature-dependent effects 5.6 imaging soft materials 5.7 Effects of ions on imaging 5.8 Imaging with a gas: summary Chapter 6 -A lab in a chamber - in situ methods in VP-ESEM and other applications 6.1 Introduction 6.2 Nanocharacterisation of insulating materials 6.3 In situ experiments 6.4 Other applications

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